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【全英文】农药兽药多组分残留质谱分析技术:第1卷.农药

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书      名:  农药兽药多组分残留质谱分析技术:第2卷.兽药(Analytical Methods for Food Safety by Mass Spectrometry:Volume Ⅱ Veterinary Drugs)
作      者:  庞国芳 著
I S B  N:  34919
完整书号:  978-7-122-34919-4
出版年份:  2019
出版月份:  11
版 / 印次:  1-1
定      价:  588.00
开      本:  16 

编辑推荐:

本书是与Elsevier合作出版项目,书中详细介绍了65项适用于动物组织(肌肉、肝脏、肾脏和脂肪)、乳制品(牛奶和奶粉)、蜂产品(蜂蜜、蜂王浆及冻干粉)、水产品(河豚鱼、鳗鱼和烤熳)及动物尿液中20类兽药残留LC-MS/MS分析方法,具有检测限低、回收率高、相对标准偏差低等特点,可满足国际食品法典委员会、欧盟、日本和美国等限量要求。作者庞国芳院士是农药及化学污染物残留分析领域的国际知名专家。


内容简介:

书是《农药兽药多组分残留质谱分析技术》的第2卷兽药篇,介绍了65项适用于动物组织(肌肉、肝脏、肾脏和脂肪)、乳制品(牛奶和奶粉)、蜂产品(蜂蜜、蜂王浆及冻干粉)、水产品(河豚鱼、鳗鱼和烤熳)及动物尿液中20类兽药残留LC-MS/MS分析方法,具有检测限低、回收率高、相对标准偏差低等特点,可满足国际食品法典委员会、欧盟、日本和美国等限量要求。各章按兽药类别,分别介绍了磺胺类、β-受体激动剂类、氨基糖苷类、氯霉素类、β-内酰胺类、大环内酯类和林可胺类、硝基呋喃类代谢物、甾体类同化激素 、非甾类同化激素类、糖皮质激素类、氟喹诺酮类、四环素类、镇静剂类、吡唑酮类、喹噁啉类、硝基咪唑类、苯并咪唑类、咪唑骈噻唑类、硫脲嘧啶类、聚醚类等20类兽药的前处理技术和测定方法,并介绍了兽药的理化性质、代谢和毒理及最大残留限量等。


作者简介:

庞国芳,中国检验检疫科学研究院,研究员,中国工程院院士,国家质检总局首席研究员、国际公职化学家联合会(AOAC)专家,国际AOAC 2014年度 Harvey W. Wiley 奖获得者。近30年一直工作在食品检验检疫一线,致力于食品科学检测技术理论与实践的研究,解决了我国相关出口食品、农产品等遭遇的技术瓶颈,为推动我国对外贸易发展做出了杰出贡献。研究制定了141项国际、国家检测技术标准。在国内、国际出版食品安全检测技术论著10部。发表论文100余篇,35篇被SCI收录。3次荣获国家科学技术进步二等奖,6次荣获国际AOAC组织颁发的科学技术奖励。


前言:

Food safety is a major security issue necessary to ensure the sound development of human society. The widespread use of pesticides, veterinary drugs, and other agricultural chemicals have contributed to widespread contamination in agricultural products. The long-term consumption of food with high residues of pesticides and veterinary drugs will cause both acute and chronic toxicity in humans and induce resistant strains, thus resulting in allergies, cancer, mutation, and teratogenicity. In order to ensure human health and food safety,countries all over the world have issued strict food safety and hygiene standards. The People’s Republic of China (PRC) has implemented strict monitoring of pesticide and veterinary drug residues, such as maximum residue limits for veterinary drugs in food of animal origin (Announcement No. 235 of the Ministry of Agriculture of the People’s Republic of China) and national food safety standards: Maximum residue limits for pesticides in food (GB 2763- 2016). The commonly used pesticides and veterinary drugs approved in China and the main agricultural products of urban residents’ daily consumption are almost all covered.
The book is a systematic summary of the high-throughput chromatographymass spectrometry technique for the analysis of multipesticides, veterinary drugs, and other agricultural chemical residues in agriculture products of plant and animal origin. Its technical characteristics are mainly embodied in the simultaneous determination of hundreds of compounds, as well as low cost and high efficiency.
This book is divided into two volumes. In Volume 1, pesticides and related chemicals are selected as the main research object, while gas chromatographymass spectrometry (GC-MS), gas chromatography-tandem mass spectrometry (GC-MS-MS), and liquid chromatography-tandem mass spectrometry (LC-MSMS) are concerned. This volume includes more than 20 analytical methods for the high-throughput analysis of multipesticide residues, and more than 1000 pesticides and related chemicals in more than 10 kinds of agricultural products and drinking water can be detected, and 400–500 kinds of pesticide residues can be detected simultaneously with the pretreatment undertaken just once. The methods for the analysis of 793 pesticides and related chemical residues in foods of plant origin applicable to fruit juices, vegetable juices, fruit wines, fruits, vegetables, cereals, tea, Chinese medicinal herbs (ramulus mori, honeysuckle, Chinese wolfberry, and lotus leaf), and edible fungi (mushroom) are introduced in Part 1; the methods for the analysis of 790 pesticides and related chemical residues in foods of animal origin applicable to honey, milk, milk powder, aquatic products (globefish, eel, and prawn), and animal muscle tissues are presented in Part 2; while the methods for the analysis of 450 pesticides and related chemical residues in drinking water are introduced in Part 3. Furthermore, the three major parameter databases adopted in the analysis of more than 1000 pesticides and related chemicals are also included in this volume: ①chromatography-mass spectrometry characteristic parameters include retention time, quantitative and qualitative ions, fragment voltage and collision energy, etc.;②performance parameters of the methods include linear equation, linear range and correlation coefficient, etc.; and③gel permeation chromatography (GPC) purification analysis parameters.
In Volume 2, the methods for the analysis of 20 species (nearly 200 kinds) of veterinary drug residues in edible animal tissues (muscle, liver, kidney, and fat), dairies (milk and milk powder), bee products (honey, royal jelly, and its lyophilized powder), aquatic products (globefish, eel, and roasted eel) and animal urine are selected as main subjects of study. The 65 analytical methods for the analysis of multiveterinary drug residues are described in different chapters by category (sulfonamides, β-adrenergic agonists, aminoglycosides, chloramphenicols,β-lactams, macrolides, nitrofurans, anabolic steroids, nonsteroidal anabolic steroids, glucocorticoids, fluoroquinolones, tetracyclines, sedatives, pyrazolones, quinoxalines, nitromidazoles, benzimidazoles, levamisole, thiourea pyrimidines, and polyethers), and 90% of the methods are LC-MS-MS. Meanwhile the physical and chemical properties, efficacy, side effects, and maximum allowable residual limit of all the compounds are also provided.
In short, this book is the summary of the work of the author team who, for more than 20 years, engaged in the research and practice of detection technology of pesticides and veterinary drug residues. These methods for the analysis of pesticides and veterinary drugs are innovative research results based on the international frontier of pesticides and veterinary drug residue analysis, and the analytical techniques adopted are new technologies widely concerned in the field of residue analysis in the world today. The performance indexes of the methods can meet the requirements of the Codex Alimentarius Commission and the world’s major developed countries; meanwhile the methods are in conformity with the developing trend of international residue analysis and they are advanced in the world. In addition, the methods established in this book have become the current effective national standard methods in China and they can be used as the detection basis of relevant testing institutions and the law basis of the relevant government departments. Nevertheless, due to the limitations of the level, there may be unavoidable errors. We would kindly ask the users of this publication to provide feedback to the authors so that subsequent editions may be improved upon.

Guo-Fang Pang


目录(节选):

Main Researchers/Editors xxvii
Preface xxix
Brief Introduction xxxi

1. Sulfonamides 1
1.1 Curative Effects and Side Effects of Sulfonamides 1
1.2 Chemical Structures and Maximum Residue Limits for Sulfonamide Drugs 2
1.3 Determination of 16 Sulfonamide Residues in Livestock and Poultry Muscles—LC-MS-MS Method (GB/T 20759-2006) 8
1.3.1 Scope 8
1.3.2 Principle 8
1.3.3 Reagents and Materials 8
1.3.4 Apparatus 9
1.3.5 Sample Pretreatment 9
1.3.6 Determination 9
1.3.7 Precision 10
1.3.8 Recovery 12
Researchers 12
Further Reading 16
1.4 Determination of 16 Sulfonamide Residues in Milk and Milk Powder—LC-MS-MS Method (GB/T 22966-2008) 16
1.4.1 Scope 16
1.4.2 Principle 16
1.4.3 Reagents and Materials 17
1.4.4 Apparatus 17
1.4.5 Sample Pretreatment 18
1.4.6 Determination 18
1.4.7 Precision 19
1.4.8 Recovery 28
Researchers 28
1.5 Determination of 18 Sulfonamide Residues in Fugu and Eel—LC-MS-MS Method (GB/T 22951-2008) 29
1.5.1 Scope 29
1.5.2 Principle 29
1.5.3 Reagents and Materials 29
1.5.4 Apparatus 30
1.5.5 Sample Pretreatment 31
1.5.6 Determination 31
1.5.7 Precision 35
1.5.8 Recovery 36
Researchers 40
1.6 Determination of 8 Sulfonamides residues in Honey—LC-FLD Method (GB/T 18932.5-2002) 41
1.6.1 Scope 41
1.6.2 Principle 41
1.6.3 Reagents and Materials 41
1.6.4 Apparatus 42
1.6.5 Sample Pretreatment 42
1.6.6 Determination 43
1.6.7 Precision 43
1.6.8 Recovery 46
Researchers 47
Further Reading 47
1.7 Determination of 16 Sulfonamide Residues in Honey—LC-MS-MS Method (GB/T 18932.17-2003) 47
1.7.1 Scope 47
1.7.2 Principle 47
1.7.3 Reagents and Materials 48
1.7.4 Apparatus 48
1.7.5 Sample Pretreatment 48
1.7.6 Determination 49
1.7.7 Precision 52
1.7.8 Recovery 52
Researchers 55
Further Reading 55
1.8 Determination of 18 Sulfonamide Residues in Royal Jelly—LC-MS-MS Method (GB/T 22947-2008) 56
1.8.1 Scope 56
1.8.2 Principle 56
1.8.3 Reagents and Materials 56
1.8.4 Apparatus 57
1.8.5 Sample Pretreatment 58
1.8.6 Determination 58
1.8.7 Precision 62
1.8.8 Recovery 64
Researchers 66

2. β-Adrenoceptor Agonists 67
2.1 Determination of 12 β-Agonist Residues in Milk and Milk Powder—LC-MS-MS Method (GB/T 22965-2008) 67
2.1.1 Scope 67
2.1.2 Principle 67
2.1.3 Reagents and Materials 68
2.1.4 Apparatus 69
2.1.5 Sample Pretreatment 69
2.1.6 Determination 70
2.1.7 Precision 76
2.1.8 Recovery 76
Researchers 78
Further Reading 78
2.2 Determination of 12 β-Agonist Residues in Fugu, Eel,and Baked Eel—LC-MS-MS Method (GB/T 22950-2008) 81
2.2.1 Scope 81
2.2.2 Principle 81
2.2.3 Reagents and Materials 81
2.2.4 Apparatus 82
2.2.5 Sample Pretreatment 83
2.2.6 Determination 84
2.2.7 Precision 85
2.2.8 Recovery 85
Researchers 85
Further Reading 88

3. Aminoglycoside 91
3.1 Curative Effects and Side Effects of Streptomycin 91
3.2 Chemical Structures and Maximum Residue Limits for Streptomycin and Dihydrostreptomycin 92
3.3 Determination of Streptomycin Residues in Honey—LC-FLD (GB/T 18932.3-2002) 93
3.3.1 Scope 93
3.3.2 Principle 93
3.3.3 Reagents and Materials 93
3.3.4 Apparatus 94
3.3.5 Sample Pretreatment 95
3.3.6 Determination 95
3.3.7 Precision 97
3.3.8 Recovery 97
Researchers 97
Further Reading 97
3.4 Determination of Streptomycin, Dihydrostreptomycin,and Kanamycin Residues in Milk and Milk
Powder—LC-MS-MS Method (GB/T 22969-2008) 98
3.4.1 Scope 98
3.4.2 Principle 98
3.4.3 Reagents and Materials 98
3.4.4 Apparatus 99
3.4.5 Preparation and Storage of Test Sample 100
3.4.6 Determination 101
3.4.7 Precision 104
3.4.8 Recovery 104
Researchers 105
3.5 Determination of Streptomycin, Dihydrostreptomycin,
and Kanamycin Residues in Fugu and Eel—LC-MS-MS Method (GB/T 22954-2008) 105
3.5.1 Scope 105
3.5.2 Principle 106
3.5.3 Reagents and Materials 106
3.5.4 Apparatus 107
3.5.5 Sample pretreatment 107
3.5.6 Determination 108
3.5.7 Precision 109
3.5.8 Recovery 110
Researchers 110
3.6 Determination of Streptomycin, Dihydrostreptomycin,
and Kanamycin Residues in Honey—LC-MS-MS Method(GB/T 22995-2008) 111
3.6.1 Scope 111
3.6.2 Principle 111
3.6.3 Reagents and Materials 111
3.6.4 Apparatus 112
3.6.5 Sample pretreatment 112
3.6.6 Determination 113
3.6.7 Precision 114
3.6.8 Recovery 115
Researchers 115
3.7 Determination of Streptomycin, Dihydrostreptomycin,
and Kanamycin Residues in Royal Jelly—LC-MS-MS Method(GB/T 22945-2008) 116
3.7.1 Scope 116
3.7.2 Principle 116
3.7.3 Reagents and Materials 116
3.7.4 Apparatus 117
3.7.5 Sample pretreatment 118
3.7.6 Determination 118
3.7.7 Precision 119
3.7.8 Recovery 120
Researchers 121

4. Chloramphenicol 123
4.1 Curative Effect and Side Effects of Chloramphenicol 123
4.2 Chemical Structures and Maximum Residue Limits for Chloramphenicol, Thiamphenicol, and Florfenicol 123
4.3 Determination of Chloramphenicol, Thiamphenicol, and Florfenicol Residues in Edible Animal Muscles, Liver, and Aquatic Products—LC-MS-MS Method (GB/T 20756-2006) 125
4.3.1 Scope 125
4.3.2 Principle 125
4.3.3 Reagents and Materials 125
4.3.4 Apparatus 126
4.3.5 Sample pretreatment 126
4.3.6 Determination 127
4.3.7 Precision 128
4.3.8 Recovery 130
Researchers 131
Further Reading 131
4.4 Determination of Chloramphenicol, Thiamphenicol, and Florfenicol Residues in Fugu, Eel, and Baked Eel—LC-MS-MSMethod (GB/T 22959-2008) 132
4.4.1 Scope 132
4.4.2 Principle 132
4.4.3 Reagents 132
4.4.4 Apparatus 133
4.4.5 Sample Pretreatment 134
4.4.6 Determination 135
4.4.7 Precision 137
4.4.8 Recovery 138
Researchers 138

5. β-Lactams 143
5.1 Curative Effects and Side Effects of Penicillins 143
5.2 Chemical Structures and Maximum Residue Limits for Penicillins 143
5.3 Determination of Nine Penicillin Residues in Livestock and Poultry Muscles — LC-MS-MS Method
(GB/T 20755-2006) 147
5.3.1 Scope 147
5.3.2 Principle 147
5.3.3 Reagents and Materials 147
5.3.4 Apparatus 148
5.3.5 Sample Pretreatment 148
5.3.6 Determination 148
5.3.7 Precision 149
5.3.8 Recovery 152
Researchers 154
Further Reading 154
5.4 Determination of Nine Penicillin Residues in Milk and Milk Powder—LC-MS-MS Method (GB/T 22975-2008) 154
5.4.1 Scope 154
5.4.2 Principle 154
5.4.3 Reagents and Materials 155
5.4.4 Apparatus and Equipment 155
5.4.5 Sample Pretreatment 156
5.4.6 Determination 156
5.4.7 Precision 159
5.4.8 Recovery 161
Researchers 162
5.5 Determination of Nine Penicillin Residues in Fugu and Eel—LC-MS-MS Method (GB/T 22952-2008) 163
5.5.1 Scope 163
5.5.2 Principle 163
5.5.3 Reagents and Materials 163
5.5.4 Apparatus 164
5.5.5 Sample Pretreatment 164
5.5.6 Determination 165
5.5.7 Precision 168
5.5.8 Recovery 170
Researchers 170
5.6 Method for the Determination of Six Penicillin Residues in Honey — LC-MS-MS Method
(GB/T 18932.25-2005) 171
5.6.1 Scope 171
5.6.2 Principle 171
5.6.3 Reagents and Materials 171
5.6.4 Apparatus 171
5.6.5 Sample Pretreatment 172
5.6.6 Determination 172
5.6.7 Precision 175
5.6.8 Recovery 177
Researchers 177
Further Reading 177
5.7 Determination of Cefapirin, Cephalexin, Cefalonium,Cefquinome Residues in Milk and Milk Powder—LC-MS-MS
Method (GB/T 22989-2008) 177
5.7.1 Scope 177
5.7.2 Principle 178
5.7.3 Reagents and Materials 178
5.7.4 Apparatus 179
5.7.5 Sample Pretreatment 179
5.7.6 Determination 180
5.7.7 Precision 182
5.7.8 Recovery 182
Researchers 184
5.8 Determination of Cefazolin, Cefapirin, Cephalexin,Cefalonium, Cefquinome Residues in Fugu and
Eel—LC-MS-MS Method (GB/T 22960-2008) 184
5.8.1 Scope 184
5.8.2 Principle 184
5.8.3 Reagents and Materials 184
5.8.4 Apparatus 185
5.8.5 Sample Pretreatment 185
5.8.6 Determination 186
5.8.7 Precision 187
5.8.8 Recovery 189
Researchers 189
5.9 Determination of Cefazolin, Cephapirin, Cephalexin,Cefalonium, Cefquinome Residues in Honey—LC-MS-MS
Method (GB/T 22942-2008) 189
5.9.1 Scope 189
5.9.2 Principle 190
5.9.3 Reagents and Materials 190
5.9.4 Apparatus 190
5.9.5 Sample Pretreatment 191
5.9.6 Determination 191
5.9.7 Precision 192
5.9.8 Recovery 194
Researchers 194

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